3-Bromothiophenol, 98% 3-溴苯硫醇
CAS 6320-01-0 MFCD00009603
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信息真实价格透明
资金保障
专业采购外包团队在线服务
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分类
- {SNA} Building Blocks, Chemical Synthesis, Organic Building Blocks, Sulfur Compounds, Thiols/Mercaptans
- {uni_hamburg} no charge; carbocycle; aromatic; 6RingOnly; 6ring; thiol; 1fragment
产品应用
- 医药中间体。
相关文献及参考
- Short: II/27B
- Short: EINECS
- Beilstein:6(4)1648
安全信息
GHS Symbol
- S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 眼睛接触后,立即用大量水冲洗并征求医生意见;
- S36/37/39 Wear suitable protective clothing, gloves and eye/face protection 穿戴适当的防护服、手套和眼睛/面保护;
- S45 In case of accident or if you feel unwell seek medical advice immediately (show the label where possible) 发生事故时或感觉不适时,立即求医(可能时出示标签);
- S23 Do not breathe gas/fumes/vapour/spray (appropriate wording to be specified by the manufacturer) 不要吸入气体/烟雾/蒸汽/喷雾;
- S60 This material and its container must be disposed of as hazardous waste 该物质及其容器必须作为危险废物处置;
- S37 Wear suitable gloves 戴适当手套;
- R36/37/38 Irritating to eyes, respiratory system and skin 对眼睛、呼吸系统和皮肤有刺激性
- R25 Toxic if swallowed 吞咽有毒
- R22 Harmful if swallowed 吞咽有害
- R34 Causes burns 会导致灼伤
- P501 Dispose of contents/container to..… 处理内容物/容器.....
- P261 Avoid breathing dust/fume/gas/mist/vapours/spray. 避免吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
- P305+P351+P338
- P260 Do not breathe dust/fume/gas/mist/vapours/spray. 不要吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
- P305+P351+P338+P310
- P310 Immediately call a POISON CENTER or doctor/physician. 立即呼救解毒中心或医生/医师。
- P280 Wear protective gloves/protective clothing/eye protection/face protection. 戴防护手套/防护服/眼睛的保护物/面部保护物。
- P271 Use only outdoors or in a well-ventilated area.? 只能在室外或通风良好的地方使用。
- P301+P330+P331+P310
- P303+P361+P353
- P270 Do not eat, drink or smoke when using this product. 使用本产品时不要吃东西,喝水或吸烟。
- H315 Causes skin irritation 会刺激皮肤
- H319 Causes serious eye irritation 严重刺激眼睛
- H335 May cause respiratory irritation 可能导致呼吸道刺激
- H302+H312+H332
其他信息
- 3-溴苯硫酚价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2014/06/02 B2348 3-溴苯硫酚 3-Bromobenzenethiol 5G 1100元 2014/06/02 B2348 3-溴苯硫酚 3-Bromobenzenethiol 25G 3400元 2010/06/21 303710050 3-溴苯硫酚 3-Bromothiophenol 95% 5 GR 1072元
- 用途一:医药中间体。
- Acros Organics:3-Bromothiophenol, 95%(6320-01-0)
- F:10-13-23
- Alfa Aesar:3-溴苯硫酚,97% 3-Bromothiophenol, 97%(6320-01-0)
- Hazard Note:Irritant/Stench
- MOL 文件:6320-01-0.mol
- 检测方法:HPLC
- Sigma Aldrich:6320-01-0(sigmaaldrich)
- 上游原料:稀硫酸 --> 间溴苯胺 --> 乙基黄原酸钾 --> 苯胺酸
- 敏感性:Stench
- 方法一:由间溴苯胺盐酸经重氮化、置换而得。将间溴苯胺酸盐、水加入反应锅,搅拌下慢慢滴加浓盐酸使全部溶解。冷却至0℃左右,缓缓滴加亚硝酸钠溶液,加毕,保温0.5h,得间溴苯胺重氮化溶液备用。另将乙基黄原酸钾水溶液加入反应锅,加热至45-50℃,缓缓加入重氮液,加毕,保温0.5h。用苯提取,提取液回收苯后,加入乙醇和氢氧化钾搅拌回流7h,回收乙醇至干,用3.6倍量的水使全部溶解,以稀硫酸调节pH至4,过滤,用苯提取,回收苯,减压蒸馏,收集120℃(2.93kPa)馏分而得成品。
- TCI Shanghai:3-溴苯硫酚 3-Bromobenzenethiol,>;98.0%(GC)(6320-01-0)