BIS(4-NITROPHENYL) CARBONATE 二(对硝基苯)碳酸酯
CAS 5070-13-3 MFCD00007322
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分类
- Active Esters/Additives, Chemical Biology, Chemical Synthesis, Coupling, Peptide Chemistry, Peptide Coupling, Synthetic Reagents
- {SNA} Active Esters/Additives, Chemical Biology, Chemical Synthesis, Coupling, Peptide Chemistry, Peptide Coupling, Synthetic Reagents
相关文献及参考
- 1. R. Glatthard, M. Matter Helv. Chim. Acta 46 , 795, (1963)
- 2. J.C. Tolle J. Am. Chem. Soc. 104 , 6883, (1982)
- 3. J. Izdebski, D. Pawlak Synthesis , 423, (1989)
- T. Wieland Justus Liebigs Ann. Chem. 655 , 189, (1962)
- B. Piekarska-Bartos., A. Temeriusz Carbohydr. Res. 203 , 302, (1990)
- Beil. 6 ,III,820
- Fieser 1 ,330
- FT-IR 1 (2), 318:A / FT-IR 2 (2), 2896:B / FT-NMR 1 (2), 1300:C / IR-Spectra (3), 1041:F / IR-Spectra (2), 911:A / NMR-Reference 2 (2), 304:C / RegBook 1 (2), 1935:E / Sigma FT-IR 1 (2), 790:B / Structure Index 1 , 311:D:3
- Reagent for peptide coupling in the presence of triethylamine in DMF, via the p-nitrophenyl active ester: Liebigs Ann. Chem., 655, 189 (1962); Helv. Chim. Acta, 46, 795 (1963). See Appendix 6.
- Has also been used as a coupling reagent in the synthesis of carbamate linked cytosine oligomers: J. Org. Chem., 52, 4202 (1987), and of ureido sugars: Carbohydr. Res., 203, 302 (1990).
安全信息
- P261 Avoid breathing dust/fume/gas/mist/vapours/spray. 避免吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
- P264 Wash hands thoroughly after handling. 处理后要彻底洗净双手。
- P280 Wear protective gloves/protective clothing/eye protection/face protection. 戴防护手套/防护服/眼睛的保护物/面部保护物。
- P302+P350
- P302+P352
- P305+P351+P338
- P305+P351+P338+P337+P313
- P321 Specific treatment (see … on this label). 具体治疗(见本标签上的)。
- P332+P313
- P337+P313
- P362 Take off contaminated clothing and wash before reuse. 脱掉污染的衣服,清洗后方可重新使用
GHS Symbol
- H315 Causes skin irritation 会刺激皮肤
- H319 Causes serious eye irritation 严重刺激眼睛
- S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 眼睛接触后,立即用大量水冲洗并征求医生意见;
- S36 Wear suitable protective clothing 穿戴适当的防护服;
- S36/37/39 Wear suitable protective clothing, gloves and eye/face protection 穿戴适当的防护服、手套和眼睛/面保护;
- R36/37/38 Irritating to eyes, respiratory system and skin 对眼睛、呼吸系统和皮肤有刺激性
- R36/38 Irritating to eyes and skin 对眼睛和皮肤有刺激性
其他信息
- 二(对硝基苯)碳酸酯价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2014/06/02 C1481 碳酸双(4-硝基苯基)酯 Bis(4-nitrophenyl) Carbonate 5G 519元 2014/06/02 C1481 碳酸双(4-硝基苯基)酯 Bis(4-nitrophenyl) Carbonate 25G 1650元 2010/05/25 L00290 双(对硝基苯)碳酸酯,98% Bis(4-nitrophenyl) carbonate, 98% 5g 473元
- 上游原料:二(三氯甲基)碳酸酯 --> 4-硝基苯酚
- TCI Shanghai:二(对硝基苯基)碳酸酯 Bis(4-nitrophenyl) Carbonate,>;97.0%(LC)(5070-13-3)
- 敏感性:Moisture Sensitive
- 存储注意事项:湿度敏感
- Sigma Aldrich:5070-13-3(sigmaaldrich)
- MOL 文件:5070-13-3.mol
- Alfa Aesar:双(对硝基苯)碳酸酯,98% Bis(4-nitrophenyl) carbonate, 98%(5070-13-3)
- F:10-21
- 检测方法:HPLC,NMR
- 图谱信息:二(对硝基苯)碳酸酯(5070-13-3)质谱(MS) 二(对硝基苯)碳酸酯(5070-13-3)红外图谱(IR1) 二(对硝基苯)碳酸酯(5070-13-3)核磁图( 13 CNMR) 二(对硝基苯)碳酸酯(5070-13-3)核磁图( 1 HNMR) 二(对硝基苯)碳酸酯(5070-13-3)红外图谱(IR2) 二(对硝基苯)碳酸酯(5070-13-3)Raman光谱